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Fundamentals of Analytical Chemistry, by Douglas A. Skoog, Donald M. West, F. James Holler
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The new edition highlights some of the latest techniques such as supercritical fluid chromatography and capillary electrophoresis. The addition of spreadsheet exercises and problems throughout the text provides students with a more modern approach to analytical chemistry.
- Sales Rank: #5361272 in Books
- Published on: 1988-03
- Original language: English
- Number of items: 1
- Binding: Hardcover
- 894 pages
Review
1. Introduction. Section I. The Tools of Analytical Chemistry. 2. Chemicals and Apparatus: Putting the Tools to Work. 3. Important Chemical Concepts: Expressing Quantities and Concentrations. 4. The Basic Approach to Chemical Equilibrium. 5. Errors in Chemical Analysis: Assessing the Quality of Results. 6. Random Errors: How Certain Can We Be? 7. Statistical Analysis: Evaluating the Data. Section II. Principles and Applications of Chemical Equilibria. 8. Gravimetric Methods of Analysis. 9. Electrolyte Effects: Activity or Concentration? 10. How Equilibrium Calculations Can Be Applied to Complex Systems. 11. Titrations: Taking Advantage of Stoichiometric Reactions. 12. Principles of Neutralization Titrations: Determining Acids, Bases, and the pH of Buffer Solutions. 13. Titrating Polyfunctional Acids and Bases. 14. Applying Neutralization Titrations. 15. Complex-Forming Titrations: Taking Advantage of Complexing Agents and Precipitating Agents. Section III. Electrochemical Methods. 16. Elements of Electrochemistry. 17. Using Electrode potentials. 18. Applying Oxidation/Reduction Titrations. 19. Potentiometry: Measuring Concentrations of Ions and Molecules. 20. A Brief Look at Some Other Electroanalytical Methods. Section IV. Spectrochemical Analysis. 21. Spectroscopic methods of Analysis: making Measurements with Light. 22. Instruments for Measuring Absorption: Is It a Photometer, a Spectrophotometer, or a Spectrometer? 23. Applying Molecular and Atomic Spectroscopic methods: Shedding More Light on the Subject. Section V. 24. An Introduction to Analytical Separations. 25. Gas-Liquid and High-Performance Liquid Chromatography. 26. Supercritical-Fluid Chromatography, Capillary Electrophoreses, and Capillary Electrochromatography. Section VI. 27. Selected Methods of Analysis. Appendix: Solubility Product Constants at 25 C. Appendix A: Acid Dissociation Constants at 25 C. Appendix B: Formation Constants of Complex Compounds at 25 C. Appendix C: Standard and Formal Electrode Potentials. Appendix D: Use of Exponential Numbers and Logarithms. Appendix E: Volumetric Calculations Using Normality and Equivalent Weight. Appendix F: Acronyms and Abbreviations of Significance in Analytical Chemistry. Appendix G: Answers to Selected Questions and Problems. Glossary. Index.
About the Author
Douglas A. Skoog (deceased) earned a B.S. in chemistry from Oregon State University and received his Ph.D. in analytical chemistry from the University of Illinois. The lead author of several best-selling texts, Dr. Skoog was the 1999 recipient of the American Chemical Society award in analytical chemistry, sponsored by the Fisher Scientific Company. That same year, he was named a Fellow of the American Association for the Advancement of Science. In 1993, he received the ACS Division of Analytical Chemistry Award for Excellence in Teaching. He was a Professor of Chemistry at Stanford University.
Donald M. West (deceased) was a Professor of Chemistry at San Jose State University.
F. James Holler is a Professor of Chemistry and recipient of the Alumni Association Great Teacher Award at the University of Kentucky. He received his Ph.D. from Michigan State University. In addition to his role as co-author of several best-selling texts, he is co-creator of the world-famous Periodic Table of Comic Books.
Stanley R. Crouch is Professor Emeritus at Michigan State University. He received his undergraduate and M.S. degrees from Stanford University and his Ph.D. in analytical chemistry from the University of Illinois. He is the recipient of the 2001 American Chemical Society Division of Analytical Chemistry Award in Chemical Instrumentation and the 1996 ACS Division of Analytical Chemistry Award for Excellence in Teaching.
Most helpful customer reviews
16 of 18 people found the following review helpful.
Good text for intro, general analytical course(s)
By Craig MACKINNON
We use this text (now in its 7th edition) for both our Analytical I (chemical analysis) and Analytical II (instrumental analysis) courses. They are both 1-semester courses at the sophomore year, and this text is just the correct level and length to cover both courses. There are a number of broad sections, each of which is divided into several chapters. Roughly the 1st half covers chemical methods and the second half covers the instrumental methods. There are also a few chapters devoted to statistical analysis.
The sections are reasonably independent and can be done in pretty much any order, giving a great degree of flexibility. The text itself is easy to read with numerous descriptive diagrams. I say this for second-year level courses - the text is too superficial for higher levels. There is a good mix of descriptive chemistry to give the student a feel for the chemistry behind the analyses. Finally, there are adequate exercises at the end of the chapters, some of which are cumulative with previous sections. There is also a very handy tutorial on the use of Microsoft's Excel for use in a course like this, including some specific exercises in using the spreadsheet. I find it very helpful, and not at all exclusive for those using Excel since Quatro-Pro (and Lotus?) is very similar and contains help files that translate from Excel parlance.
My biggest issue is lack of a section on mass spectroscopy. Skoog's own "Instrumental Analysis" text has a fine section on mass spec, but this text contains virtually no mention of the technique, in spite of the fact that it is an increasingly important technique for both quantitative and qualitative trace analysis. However, that's the only real negative point - this text is very good and useful for 2nd year level analytical courses. (P.S. students find it straightforward and clear as well.)
23 of 25 people found the following review helpful.
A Worthy Alternative to Skoog and West's Fundamentals of...
By A Customer
This text is a worthy contender to the classic "Fundamentals of Analytical Chemistry' by Skoog and West. I feel it is easier to read, and the examples given in the inserts should provide students with a "real world" need for the topics covered. The coverage is very similar to Fundamentals of Analytical Chemistry. The example problems and homework problems are illustrative and challanging. The experiments presented in the final chapters are well documented. My only observations for improvement would be the use of more detailed analysis of some of the insert examples. For example, a battery technology that is discussed in a step by step fashion in terms of equilibria, balancing redox equations, and problem solving. Also, a modernization of laboratory experiments to include topics in biochemistry, food and environmental science would be helpful in any future editon.
3 of 3 people found the following review helpful.
Analytical Chemistry: an introduction
By Stephen Patton
This book is definetly a keeper! A masterpiece of clarity. Although it is >10 years old, this introductory book is still by far the best book of its kind. It is one of of the few chemistry books that I have read from cover to cover several times, and each time I still pick up insights into problem solving and the reasoning behind analytical techniques. The classical experiments in chapter 27 are so good that purchase of a seperate laboratory book is un-necessary.
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